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Precision and Accuracy in Elemental Determination in Environmental Samples Using Instrumental Neutron Activation Analysis


Article Information

Title: Precision and Accuracy in Elemental Determination in Environmental Samples Using Instrumental Neutron Activation Analysis

Authors: Shamshad Begum Quraishi, Chung Yong- Sam

Journal: Pakistan Journal of Scientific and Industrial Research (Series B: Biological Sciences)

HEC Recognition History
Category From To
Y 2023-07-01 2024-09-30
Y 2022-07-01 2023-06-30
Y 2021-07-01 2022-06-30
Y 2020-07-01 2021-06-30
Y 1900-01-01 2005-06-30

Publisher: PCSIR Scientific Information Centre

Country: Pakistan

Year: 2005

Volume: 48

Issue: 3

Language: English

Keywords: elemental analysisenvironmental elementsprecision analysisenvironmental contaminationinstrumental neutron activation analysisINAA

Categories

Abstract

Thirty elements were determined in different environmental certified reference materials (CRMs) with high accuracy and precision using instrumental neutron activation analysis (INAA). The relative error of most of the elements was found to be within 10% and the standard deviation was less than 15%. The Z-score, as an analytical performance indicator, was also less than ±2. The accourate determination of various trace and major elements, at extremely low concentrations, usually present in very small amounts of airborne particulate matter on filter media was performed satisfactorily by INAA, which is otherwise regarded as a problem in such determinations. On the other hand, nevertheless, INAA appeared to be an inadequate method for the analysis of Ca because of the low count rate.


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