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Mechanical design for high-pressure reactor to microwave-assisted leaching of refractory metals


Article Information

Title: Mechanical design for high-pressure reactor to microwave-assisted leaching of refractory metals

Authors: Vera E. D., Peña C. A., Bolívar R.

Journal: ARPN Journal of Engineering and Applied Sciences

HEC Recognition History
Category From To
Y 2023-07-01 2024-09-30
Y 2022-07-01 2023-06-30
Y 2021-07-01 2022-06-30
X 2020-07-01 2021-06-30

Publisher: Khyber Medical College, Peshawar

Country: Pakistan

Year: 2022

Volume: 17

Issue: 3

Language: English

Categories

Abstract

The Colombian platinic alluvium metal contains platinum, iridium, osmium and palladium. Iridium and osmium confer a refractory condition that makes the leaching of the alluvium very difficult. This is the first aspect to be solved in the development of a refining process. Acid microwave-assisted leaching offers a higher leaching rate with high recovery levels, so it seems a possible way to solve this problem. A low-cost reactor to microwave-assisted leaching process has been designed using section VIII ASME code, comparison with commercial reactors and both SolidWorks and Ces-Edupack CAE. The 180 ml reactor was design take in account a high pressure of 8.3 MPa (1200 psi), 180°C temperature, chemical resistance to aqua regia, hydrochloric and hydro nitric acid and ergonomic and safety demands.


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