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Synthesis and Characterization of Some Metal Complexes Derived from Azo Ligand of 4,4' Methylenedianiline and Resorcinol


Article Information

Title: Synthesis and Characterization of Some Metal Complexes Derived from Azo Ligand of 4,4' Methylenedianiline and Resorcinol

Authors: Lina Saadi, Azhar A. Ghali

Journal: Biomedicine and chemical sciences

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Year: 2022

Volume: 1

Issue: 4

Language: en

DOI: 10.48112/bcs.v1i4.252

Keywords: spectral methodsresorcinol4,4ʹ-methylenedianilineAzodye

Categories

Abstract

The metal complexes of Azo dye; 4,4'-((methylene bis(3,l-phenylen)) bis (diazene-l,2-diyl)) bis(1,3-Benzenediol) are produced from 4,4`- methylenedianiline and Resorcinol were synthesized and characterized by using several analytical and spectral techniques. The ligand and its complexes were characterized by many chemo-physic methods like NMR, IR, UV-Vis, molar conductance measurement, analytical measurement, and melting point. The conditions of optimal reaction  (for instance reagent concentration, pH etc) were studied and the analytical figures of merit such as limit of detection, linearity, sensitivity etc) were obtained.


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