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An investigation of Y-TZP surface characteristics and adhesive properties following treatment with Tri-biochemical Silica Coating, Femtosecond Laser, and Nano-hydroxyapatite: A scanning electron microscopy evaluation


Article Information

Title: An investigation of Y-TZP surface characteristics and adhesive properties following treatment with Tri-biochemical Silica Coating, Femtosecond Laser, and Nano-hydroxyapatite: A scanning electron microscopy evaluation

Authors: Fahad Alkhudhairy, Nourah N. Shono

Journal: Pakistan Journal of Medical Sciences

HEC Recognition History
Category From To
Y 2024-10-01 2025-12-31
X 2023-07-01 2024-09-30
X 2022-07-01 2023-06-30
X 2021-07-01 2022-06-30
X 2020-07-01 2021-06-30
W 2009-07-01 2020-06-30
Z 2006-11-07 2009-07-01
Y 1900-01-01 2005-06-30

Publisher: Professional Medical Publications

Country: Pakistan

Year: 2025

Volume: 41

Issue: 3

Language: en

DOI: 10.12669/pjms.41.3.11302

Keywords: Femtosecond laserTribochemical silica coatingNano-hydroxyapatite coatingAir-particle abrasionDentistryMechanical testingSurface ModificationSurface characteristicsShear bond strengthZirconia Polycrystals

Categories

Abstract

Objectives: To examine how advanced surface pretreatment techniques - Tribochemical silica coating (TBC), Femtosecond laser (FS), and Nano-hydroxyapatite (HA) coating - affect the surface roughness (Ra) and shear bond strength (SBS) between resin luting cement and Yttria-stabilized tetragonal zirconia polycrystals (Y-TZP)
Methods: The lab-based comparative study was approved by the ethical committee of King Saud University under IRB number F98-971X9 and was completed in three months (June to September, 2024). Eighty-four YTZP zirconia discs were created and sorted into four groups based on different conditioning agents: Group-I (APA) as the control, Group-II (TBC), Group-III (FS laser), and Group-IV (Nano-HA coating). Ra was measured on five discs from each group using a profilometer, while surface topography was examined through SEM analysis. Ten specimens per group were bonded with luting cement, followed by SBS testing and fracture mode analysis using a universal testing machine and stereomicroscope, respectively. One-way ANOVA with post hoc Tukey tests (p<0.05) was used for statistical analysis of Ra and SBS means across the groups.
Results: Group-IV (Nano-HA coating) exhibited the highest Ra and SBS values. Conversely, Group II (TBC) displayed the lowest Ra and weakest bond strength.
Conclusion: Nano-HA coating and FS laser can be employed as viable alternatives to APA without compromising the physical and mechanical properties of zirconia ceramic.
doi: https://doi.org/10.12669/pjms.41.3.11302
How to cite this: Alkhudhairy F, Shono NN. An investigation of Y-TZP surface characteristics and adhesive properties following treatment with Tri-biochemical Silica Coating, Femtosecond Laser, and Nano-hydroxyapatite: A scanning electron microscopy evaluation. Pak J Med Sci. 2025;41(3):758-762. doi: https://doi.org/10.12669/pjms.41.3.11302
This is an Open Access article distributed under the terms of the Creative Commons Attribution License (http://creativecommons.org/licenses/by/3.0), which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.


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